Nmr And Macromolecules

NMR and Macromolecules PDF
Author: James C. Randall
Publisher: Amer Chemical Society
ISBN: 9780841208292
Size: 68.63 MB
Format: PDF, Kindle
Category : Science
Languages : en
Pages : 280
View: 4996

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High Resolution Nmr Of Macromolecules

High Resolution NMR of Macromolecules PDF
Author: Frank Bovey
Publisher: Elsevier
ISBN: 032314893X
Size: 55.65 MB
Format: PDF, Docs
Category : Science
Languages : en
Pages : 476
View: 5599

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High Resolution NMR of Macromolecules presents the development in the NMR study of polymers. This book discusses the exciting area of application of NMR to polymer science as the result of the more general accessibility of instruments of high magnetic field. Organized into 15 chapters, this book begins with an overview of the spectral analysis and the dependence of chemical shifts and J couplings on structure. This text then discusses the isomerism in polymer chains without special reference to NMR. Other chapters consider the interpretation of synthetic polymer spectra in terms of structure, stereochemical configuration, conformation, and chain growth mechanism. This book discusses as well the application of high resolution NMR to the study of nucleic acids, which has not been so well developed as that of polypeptides and proteins. The final chapter deals with biopolymers and their model compounds. This book is a valuable resource for chemists and research workers.

Nmr And Macromolecules

NMR and Macromolecules PDF
Author: James C. Randall
Publisher: Amer Chemical Society
ISBN: 9780841208292
Size: 65.88 MB
Format: PDF, ePub
Category : Science
Languages : en
Pages : 280
View: 4720

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Chain Structure And Conformation Of Macromolecules

Chain Structure and Conformation of Macromolecules PDF
Author: Frank Bovey
Publisher: Elsevier
ISBN: 0323158439
Size: 69.22 MB
Format: PDF
Category : Science
Languages : en
Pages : 270
View: 2043

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Chain Structure and Conformation of Macromolecules provides an introduction to the chain structures of synthetic polymers and their determination in solution and in the solid state. This book discusses the synthetic methods and polymerization mechanisms. Organized into eight chapters, this book begins with an overview of the brief history of the macromolecular concept and of stereochemical and geometrical isomerism in synthetic polymer chains. This text then introduces vibrational spectroscopy and nuclear magnetic resonance spectroscopy. Other chapters consider the geometric isomerism in diene copolymers as well as the rotational isomeric state method of calculation of polymer chain dimensions. This book discusses as well copolymerization and the measurement of copolymer structure. The final chapter deals with the NMR observation of polymers in the solid state by the method of magic angle spinning, by which both dynamic measurements and high resolution structural information are possible. This book is a valuable resource for organic chemists, chemical engineers, and research workers.

Nmr As A Structural Tool For Macromolecules

NMR as a Structural Tool for Macromolecules PDF
Author: M.D. Kemple
Publisher: Springer Science & Business Media
ISBN: 1461303877
Size: 60.15 MB
Format: PDF
Category : Science
Languages : en
Pages : 400
View: 3188

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The contemplation of truth and beauty is the proper object for which we were created, which calls forth the most intense desires of the soul, and of which it never tires -Hazlitt In his Nobel lecture Purcell commented that when he saw snow in New England after the discovery of NMR, it appeared like "heaps of protons quietly precessing in earth's magnetic field. " If he were to make the comment in the context of how NMR is being used today, he could have conjured up an image of hydrogen, carbon, and nitrogen nuclei in proteins of an earthbound 8rganism subtly orchestrating a quiet symphony of frequencies, from 150 Hz to 2 kHz, carrying clues to the three-dimensional structure of the macromolecules. The manner in which the basic discoveries of Bloch and Purcell have led to the emergence of NMR, several decades later, as a major technique of biological and medical physics (and chemistry) is a striking example of the power of basic research. It is also a fascinating saga whereby whenever it was felt that the field had reached a plateau, new directions, new technologies, and sometimes serendipity produced new developments that revolutionized the technique and enhanced its capability. As Richard Ernst points out "NMR is intellectually attractive, . . . the practical importance of NMR is enormous, and can justify much of the playful activities of an addicted spectroscopist" (Nobel lecture).

Molecular Structure And Dynamics

Molecular Structure and Dynamics PDF
Author:
Publisher: Academic Press
ISBN: 9780080859989
Size: 16.94 MB
Format: PDF, ePub, Docs
Category : Science
Languages : en
Pages : 589
View: 7716

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Molecular Structure and Dynamics

Nmr Spectroscopy And Its Application To Biomedical Research

NMR Spectroscopy and its Application to Biomedical Research PDF
Author: S.K. Sarkar
Publisher: Elsevier
ISBN: 9780080537597
Size: 41.70 MB
Format: PDF, Kindle
Category : Science
Languages : en
Pages : 387
View: 2884

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NMR has become the most diverse spectroscopic tool available to date in biomedical research. It is now routinely used to study biomolecular structure and dynamics particularly as a result of recent developments of a cascade of highly sophisticated multidimensional NMR pulse sequences, and of advances in genetic engineering to produce biomolecules, uniformly or selectively enriched with 13C, 15N and 2H. Features of this book: • Provides an up-to-date treatment of NMR techniques and their application to problems of biomedical interest • Most refined multidimensional pulse sequences including the basic aspects are covered by leading NMR spectroscopists. The book will be useful to NMR spectroscopists, biochemists, and to molecular biologists interested in the use of NMR techniques for solving biological problems.

Nuclear Magnetic Resonance Of Biological Macromolecules

Nuclear Magnetic Resonance of Biological Macromolecules PDF
Author:
Publisher: Elsevier
ISBN: 0080496881
Size: 55.77 MB
Format: PDF
Category : Science
Languages : en
Pages : 480
View: 7141

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This volume and its companion, Volume 339, supplement Volumes 176, 177, 239, and 261. Chapters are written with a "hands-on" perspective. That is, practical applications with critical evaluations of methodologies and experimental considerations needed to design, execute, and interpret NMR experiments pertinent to biological molecules.

Nuclear Magnetic Resonance

Nuclear Magnetic Resonance PDF
Author: G. A. Webb
Publisher: Royal Society of Chemistry
ISBN: 0854043225
Size: 71.36 MB
Format: PDF, Mobi
Category : Reference
Languages : en
Pages : 550
View: 6061

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For those wanting to become rapidly acquainted with specific areas of NMR, this title provides unrivalled scope of coverage.

Nuclear Magnetic Resonance

Nuclear Magnetic Resonance PDF
Author: Royal Society of Chemistry (Great Britain)
Publisher: Royal Society of Chemistry
ISBN: 9780854043422
Size: 72.52 MB
Format: PDF, ePub, Mobi
Category : Reference
Languages : en
Pages : 586
View: 3318

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For those wanting to become rapidly acquainted with specific areas of NMR, this title provides unrivalled scope of coverage.

Protein Nmr Spectroscopy

Protein NMR Spectroscopy PDF
Author: John Cavanagh
Publisher: Elsevier
ISBN: 9780080471037
Size: 61.62 MB
Format: PDF
Category : Science
Languages : en
Pages : 912
View: 5163

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Protein NMR Spectroscopy, Second Edition combines a comprehensive theoretical treatment of NMR spectroscopy with an extensive exposition of the experimental techniques applicable to proteins and other biological macromolecules in solution. Beginning with simple theoretical models and experimental techniques, the book develops the complete repertoire of theoretical principles and experimental techniques necessary for understanding and implementing the most sophisticated NMR experiments. Important new techniques and applications of NMR spectroscopy have emerged since the first edition of this extremely successful book was published in 1996. This updated version includes new sections describing measurement and use of residual dipolar coupling constants for structure determination, TROSY and deuterium labeling for application to large macromolecules, and experimental techniques for characterizing conformational dynamics. In addition, the treatments of instrumentation and signal acquisition, field gradients, multidimensional spectroscopy, and structure calculation are updated and enhanced. The book is written as a graduate-level textbook and will be of interest to biochemists, chemists, biophysicists, and structural biologists who utilize NMR spectroscopy or wish to understand the latest developments in this field. Provides an understanding of the theoretical principles important for biological NMR spectroscopy Demonstrates how to implement, optimize and troubleshoot modern multi-dimensional NMR experiments Allows for the capability of designing effective experimental protocols for investigations of protein structures and dynamics Includes a comprehensive set of example NMR spectra of ubiquitin provides a reference for validation of experimental methods

Nuclear Magnetic Resonance

Nuclear Magnetic Resonance PDF
Author: R. K. Harris
Publisher: Royal Society of Chemistry
ISBN: 0851862721
Size: 12.31 MB
Format: PDF
Category : Medical
Languages : en
Pages : 440
View: 3207

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For those wanting to become rapidly acquainted with specific areas of NMR, this title provides unrivalled scope of coverage.